HCID 14770215, compound → HCID 20065872, compound

HRID 359223Notes

Reaction equation

HRID 359223 reaction equation
[Br:1]CC1C2C(C=CC=1)=CC1C3C=CC=CC=3OC=1C=2.[CH3:20][C:21]1[C:29]2[C:28]3[CH:30]=[C:31]4[C:36](=[CH:37][C:27]=3[O:26][C:25]=2[CH:24]=[CH:23][CH:22]=1)[CH:35]=[CH:34][CH:33]=[CH:32]4>>[Br:1][CH2:20][C:21]1[C:29]2[C:28]3[CH:30]=[C:31]4[C:36](=[CH:37][C:27]=3[O:26][C:25]=2[CH:24]=[CH:23][CH:22]=1)[CH:35]=[CH:34][CH:33]=[CH:32]4

Participants

3

Reactant 2

HCID 14770215HCID 14770215, compoundHCID 20065958HCID 20065958, compound

Product 1

HCID 20065872HCID 20065872, compoundYield 72%

Procedure

Using the procedure outlined in 6A, 1-methylbenzo[b]naphtho[2,3-d]furan (Cambridge Chemicals, Inc.) gave 72% yield of crude 1-bromomethylbenzo[b]naphtho[2,3-d]furan which was used without further purification.

Sources & evidence

ORD record
ord-cdf354cbe4b34d28ade74fa6e59ca451
Source dataset
uspto-grants-1991_03
Patent number
US04999369

Reaction notes

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