HCID 14770221, compound → HCID 20065845, compound

HRID 359228Notes

Reaction equation

HRID 359228 reaction equation
C1C2C3C=[C:11]4[C:16](=CC=3SC=2C=CC=1)[CH:15]=[C:14]([CH:18]=[O:19])[CH:13]=[CH:12]4.[CH2:20]([N:22]1[C:34]2[CH:33]=[CH:32][C:31]3[CH:35]=[CH:36][CH:37]=[CH:38][C:30]=3[C:29]=2C2C=CC=C(C)C1=2)[CH3:21]>C(Cl)Cl.CCCCCC>[CH2:20]([N:22]1[C:34]2[CH:33]=[CH:32][C:31]3[CH:35]=[CH:36][CH:37]=[CH:38][C:30]=3[C:29]=2[C:16]2[C:15]1=[C:14]([CH:18]=[O:19])[CH:13]=[CH:12][CH:11]=2)[CH3:21]

Participants

4

Reactant 2

HCID 14770221HCID 14770221, compoundHCID 20065879HCID 20065879, compound

Product 1

HCID 20065845HCID 20065845, compoundYield 17.2%

Reagents, catalysts & solvents 1

HCID 21226440Methylenechloride HexaneSolvent

Procedure

Using the procedure outlined in 8A, 7-ethyl-8-methyl-7H-benzo[c]carbazole gave a 17.2% of 7-ethyl-7H-benzo[c]carbazole-8-carbaldehyde, mp 148°-149°, (CH2Cl2 /hexane), (C,H,N).

Sources & evidence

ORD record
ord-94fcd2aef48549f19e2ebbe1e9a6c19c
Source dataset
uspto-grants-1991_03
Patent number
US04999369

Reaction notes

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