HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzo(b)naphtho(1,2-d)thiophene, 10-methyl- → HCID 20065910, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzo(b)naphtho(1,2-d)thiophene, 10-methyl- | HCID 150076 | — |
| Reactant | HCID 14770215 | HCID 14770215 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 20065910 | HCID 20065910 | 39% |
Reaction Steps
Using the procedure outlined in 6A, 10-methyl-benzo[b]naphtho[1,2-d]thiophene (H. G. Pars Pharmaceutical Laboratories, Inc.) gave a 39.0% yield of 10-(bromomethyl)-benzo[b]naphtho[1,2-d]thiophene, mp 202°-203°, (CH2Cl2), (C,H,Br,S).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04999369 |
| Source dataset | uspto-grants-1991_03 |
| ORD ID | ord-8d43c7809be241c1959f31e798308566 |
| Source note | uspto-grants-1991_03 |