Urea, tricyclo(3.3.1.1(sup 3,7))dec-1-yl- → HCID 20064724, compound

Participants

Reaction Steps

By the procedure of Example 4, 11.6 g (60 mmol) of adamantyl urea was reacted with 10.9 g (50 mmol) of ethyl 2-chloro-4,4,4-trifluoroacetoacetate at 140°-150° C. for 24 hours. The product was separated and then recrystallized from methylcyclohexane to yield 7.0 g of a white solid product (m.p.=109°-111° C.) identified in Table I.

Provenance & Evidence