Benzoyl chloride → HCID 18963390, compound

HRID 359318Notes

Reaction equation

HRID 359318 reaction equation
[C:1]([C:4]1[CH2:9][CH2:8][CH2:7][NH:6][CH:5]=1)(=[O:3])[CH3:2].[C:10](Cl)(=[O:17])[C:11]1[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=1.CC(N1CCCC(C(C)=O)=C1)C>>[C:10]([N:6]1[CH2:7][CH2:8][CH2:9][C:4]([C:1]([CH3:2])=[O:3])=[CH:5]1)(=[O:17])[C:11]1[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=1

Participants

4

Reactant 3

HCID 7412Benzoyl chlorideHCID 32845951-(1,4,5,6-tetrahydropyridin-3-yl)ethanoneHCID 18963350HCID 18963350, compound

Product 1

HCID 18963390HCID 18963390, compound

Procedure

Methyl 1-benzoyl-1,4,5,6-tetrahydro-3-pyridyl ketone was prepared from 3-acetyl-1,4,5,6-tetrahydropyridine and benzoyl chloride according to the procedure of Part (b) of Example 1. The product was recrystallised from ethanol/water m.pt. 93-95°C.

Workup

  1. customThe product was recrystallised from ethanol/water m.pt. 93-95°C.

Sources & evidence

ORD record
ord-3f66452c44f6498ab521b8d027f8a805
Source dataset
uspto-grants-1991_03
Patent number
US05000946

Reaction notes

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