HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Butyl-3-butyryl pyridinium bromide → Propyl 1-butyl-1,4,5,6-tetrahydro-3-pyridyl ketone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Butyl-3-butyryl pyridinium bromide | HCID 18963352 | — |
| Reactant | Methyl 1-(2-phenylethyl)-1,4,5,6-tetrahydro-3-pyridyl ketone | HCID 18963355 | — |
| Product | Propyl 1-butyl-1,4,5,6-tetrahydro-3-pyridyl ketone | HCID 18963360 | — |
Reaction Steps
1-Butyl-3-butyryl pyridinium bromide was hydrogenated according to the procedure described in Part (b) of Example 6 to give propyl 1-butyl-1-4,5,6-tetrahydro-3-pyridyl ketone (13). The product was distilled as a pale yellow oil (b.pt. 120-124°C./0.02 mm Hg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05000946 |
| Source dataset | uspto-grants-1991_03 |
| ORD ID | ord-4b8d68bd7cfd4206b68985ff1bc37ff8 |
| Source note | uspto-grants-1991_03 |