HCID 18963355, compound → Propyl 1-(3-methylbutyl)-1,4,5,6-tetrahydro-3pyridyl ketone

HRID 359328Notes

Reaction equation

HRID 359328 reaction equation
[Cl-].[CH3:2][C:3]([CH3:17])=[CH:4][CH2:5][N+:6]1[CH:11]=[CH:10][CH:9]=[C:8]([C:12](=[O:16])[CH2:13][CH2:14][CH3:15])[CH:7]=1.C1(CCN2CCCC(C(C)=O)=C2)C=CC=CC=1>>[CH3:2][CH:3]([CH3:17])[CH2:4][CH2:5][N:6]1[CH2:11][CH2:10][CH2:9][C:8]([C:12]([CH2:13][CH2:14][CH3:15])=[O:16])=[CH:7]1

Participants

3

Reactant 2

HCID 18963355HCID 18963355, compoundHCID 189633791-(3-Methyl-2-butenyl)-3-butyryl pyridinium chloride

Product 1

HCID 17914315Propyl 1-(3-methylbutyl)-1,4,5,6-tetrahydro-3pyridyl ketone

Procedure

1-(3-Methyl-2-butenyl)-3-butyryl pyridinium chloride was hydrogenated according to the procedure described in Part (b) of Example 6 to give propyl 1-(3-methylbutyl)-1,4,5,6-tetrahydro-3-pyridyl ketone (14). The product was distilled as a pale yellow oil (b.pt. 126-129°C./0.02 mm Hg).

Sources & evidence

ORD record
ord-4edb605d065240278485cd3459fb4d03
Source dataset
uspto-grants-1991_03
Patent number
US05000946

Reaction notes

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