m-Anisoyl chloride → HCID 18963378, compound

HRID 359335Notes

Reaction equation

HRID 359335 reaction equation
[CH3:1][C:2]1([CH3:13])[CH2:11][C:10]2[NH:9][CH2:8][CH2:7][CH2:6][C:5]=2[C:4](=[O:12])[CH2:3]1.[CH3:14][O:15][C:16]1[CH:17]=[C:18]([CH:22]=[CH:23][CH:24]=1)[C:19](Cl)=[O:20].CC(N1CCCC(C(C)=O)=C1)C>>[CH3:1][C:2]1([CH3:13])[CH2:11][C:10]2[N:9]([C:19](=[O:20])[C:18]3[CH:22]=[CH:23][CH:24]=[C:16]([O:15][CH3:14])[CH:17]=3)[CH2:8][CH2:7][CH2:6][C:5]=2[C:4](=[O:12])[CH2:3]1

Participants

4

Reactant 3

HCID 74374m-Anisoyl chlorideHCID 118196217,7-Dimethyl-2,3,4,6,7,8-hexahydroquinolin-5(1H)-oneHCID 18963350HCID 18963350, compound

Product 1

HCID 18963378HCID 18963378, compound

Procedure

7,7-Dimethyl-1,2,3,4,7,8-hexahydro-quinolin5(6H)-one was reacted with 3-methoxybenzoyl chloride according to the procedure of Part (b) of Example 1 to give 7,7-dimethyl-1,2,3,4, 7,8-hexahydro-1-(3-methoxybenzoyl)-quinolin-5(6H)-one (20) as a pale yellow solid.

Sources & evidence

ORD record
ord-0ca3b4aaa20c4c368a8e143c417f9e84
Source dataset
uspto-grants-1991_03
Patent number
US05000946

Reaction notes

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