p-Anisoyl chloride → HCID 18963369, compound

HRID 359336Notes

Reaction equation

HRID 359336 reaction equation
[CH3:1][C:2]1([CH3:13])[CH2:11][C:10]2[NH:9][CH2:8][CH2:7][CH2:6][C:5]=2[C:4](=[O:12])[CH2:3]1.[CH3:14][O:15][C:16]1[CH:24]=[CH:23][C:19]([C:20](Cl)=[O:21])=[CH:18][CH:17]=1>>[CH3:1][C:2]1([CH3:13])[CH2:11][C:10]2[N:9]([C:20](=[O:21])[C:19]3[CH:23]=[CH:24][C:16]([O:15][CH3:14])=[CH:17][CH:18]=3)[CH2:8][CH2:7][CH2:6][C:5]=2[C:4](=[O:12])[CH2:3]1

Participants

3

Reactant 2

HCID 7477p-Anisoyl chlorideHCID 118196217,7-Dimethyl-2,3,4,6,7,8-hexahydroquinolin-5(1H)-one

Product 1

HCID 18963369HCID 18963369, compound

Procedure

7,7-Dimethyl-1,2,3,4,7,8-hexahydro-quinoline-5(6H)-one was reacted with 4-methoxybenzoyl chloride according to the procedure of Part b) of Example 1 to give 7,7-dimethyl-1,2,3,4, 7,8-hexahydro-1-(4-methoxybenzoyl)-quinoline5(6H)-one (21) as a yellow waxy solid.

Sources & evidence

ORD record
ord-bf5e72d87a3a4bb285606c1c75bd5643
Source dataset
uspto-grants-1991_03
Patent number
US05000946

Reaction notes

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