HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetone → 4-(4,4-Dimethyl 3-(2-methoxyethyl) 5-oxo 2-thioxo 1-imidazolidinyl) 2-(trifluoromethyl) benzonitrile
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetone | HCID 180 | — |
| Reactant | Dichloromethane | HCID 6344 | — |
| Reactant | HCID 22116964 | HCID 22116964 | — |
| Product | 4-(4,4-Dimethyl 3-(2-methoxyethyl) 5-oxo 2-thioxo 1-imidazolidinyl) 2-(trifluoromethyl) benzonitrile | HCID 22116949 | — |
Reaction Steps
Using the procedure of Example 71, the product of Example 78 was reacted to obtain the expected product melting at 98°-99° C. with a Rf=0.32 (eluant: methylene chloride--acetone (99-1))
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05411981 |
| Source dataset | uspto-grants-1995_05 |
| ORD ID | ord-4590a017bb1c4bf6a61356fbcebbdbba |
| Source note | uspto-grants-1995_05 |