HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Acetone Cyanohydrin → 2-((4-Hydroxybutyl)amino)-2-methylpropanenitrile
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Acetone Cyanohydrin | HCID 6406 | — |
| Edukt | 4-Amino-1-butanol | HCID 25868 | — |
| Lösungsmittel | Dichloromethane | HCID 6344 | — |
| Produkt | 2-((4-Hydroxybutyl)amino)-2-methylpropanenitrile | HCID 15511961 | — |
Reaktionsbedingungen
| Temperatur | 20 °C |
|---|
Reaktionsschritte
220 μl of acetone cyanohydrin and 200 μl of 4-amino 1-butanol were mixed together with stirring for 16 hours at 20° C. and then was diluted with 2 ml of methylene chloride, dried, filtered and the filtrate was concentrated under reduced pressure to obtain the propanonitrile which was used as is for the following stage.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05411981 |
| Quelldatensatz | uspto-grants-1995_05 |
| ORD ID | ord-af507ea0ea16417b8b65e6f6abd9ae52 |
| Quellennotiz | uspto-grants-1995_05 |