Pyridine → HCID 15135635, compound

HRID 359477Notes

Reaction equation

HRID 359477 reaction equation
[NH2:1][C:2]1[C:7]([C:8](=[O:14])[C:9]2[S:13][CH:12]=[CH:11][CH:10]=2)=[CH:6][CH:5]=[CH:4][N:3]=1.[Br:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][C:21](Cl)=[O:22].N1C=CC=CC=1>ClC(Cl)C>[Br:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][C:21]([NH:1][C:2]1[C:7]([C:8](=[O:14])[C:9]2[S:13][CH:12]=[CH:11][CH:10]=2)=[CH:6][CH:5]=[CH:4][N:3]=1)=[O:22]

Participants

5

Reactant 3

HCID 1049PyridineHCID 898486-Bromohexanoyl chlorideHCID 12711132HCID 12711132, compound

Product 1

HCID 15135635HCID 15135635, compound

Reagents, catalysts & solvents 1

HCID 63651,1-DichloroethaneSolvent

Procedure

2-Amino-3-(2-thenoyl)pyridine is reacted with 6-bromohexanoyl chloride in the presence of pyridine in dichloroethane to give 2-(6-bromohexanoylamino)-3-(2-thenoyl)pyridine.

Sources & evidence

ORD record
ord-91513e682d2d4490b7e6d970152b5418
Source dataset
uspto-grants-1991_03
Patent number
US05001137

Reaction notes

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