HuagongsheHuagongshe Chemistry Print Report · For research reference only
Anthranilamide → HCID 730237, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Anthranilamide | HCID 6942 | — |
| Reactant | Benzoyl isothiocyanate | HCID 68284 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 730237 | HCID 730237 | 95% |
Reaction Steps
To a stirred mixture of 13.6 g of 2-aminobenzamide and 200 ml of ether Was added dropwise, a solution of 16.3 g of benzoyl isothiocyanate in 100 ml of ether over 30 minutes. After standing 48 hours, the solid Was collected, giving 28.4 g of the desired product as grey crystals, mp 190°-192° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05001157 |
| Source dataset | uspto-grants-1991_03 |
| ORD ID | ord-76d35e2a2afa429996c67452b593be6b |
| Source note | uspto-grants-1991_03 |