Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Anthranilamide → N-[(2-carbamoylphenyl)carbamothioyl]-4-methylbenzamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Anthranilamide | HCID 6942 | — |
| 반응물 | 4-Methylbenzoyl isothiocyanate | HCID 140139 | — |
| 용매 | Diethyl Ether | HCID 3283 | — |
| 생성물 | N-[(2-carbamoylphenyl)carbamothioyl]-4-methylbenzamide | HCID 667640 | 98.2% |
반응 단계
To a stirred mixture of 5.4 g of 2-aminobenzamide and 200 ml of ether was added dropwise, a solution of 7.5 g of 4-methylbenzoyl isothiocyanate in 100 ml of ether over 30 minutes. After 48 hours, the solid was collected, giving 12.2 g of the desired product as grey crystals, mp 208°-210° C. (dec.).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05001157 |
| 출처 데이터셋 | uspto-grants-1991_03 |
| ORD ID | ord-86efcdbdb17b4b80a7e95de09395ece8 |
| 출처 메모 | uspto-grants-1991_03 |