HuagongsheHuagongshe Chemistry Print Report · For research reference only
Anthranilamide → 2-[(4-Methoxybenzoyl)carbamothioylamino]benzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Anthranilamide | HCID 6942 | — |
| Reactant | 4-Methoxybenzoyl isothiocyanate | HCID 140136 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | 2-[(4-Methoxybenzoyl)carbamothioylamino]benzamide | HCID 892814 | 833% |
Reaction Steps
To a stirred mixture of 7.5 g of 2-aminobenzamide and 150 ml of ether was added dropwise, a mixture of 1.0 g of 4-methoxybenzoyl isothiocyanate in ether over 15 minutes. After stirring overnight, the solid was collected, giving 14.2 g of the desired product as grey crystals, mp 193°-196° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05001157 |
| Source dataset | uspto-grants-1991_03 |
| ORD ID | ord-b5eb73a0104f4a2696ff74b22d8f3ea4 |
| Source note | uspto-grants-1991_03 |