HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzoyl isothiocyanate → HCID 15135530, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzoyl isothiocyanate | HCID 68284 | — |
| Reactant | 2-Amino-4,5-dimethoxybenzamide | HCID 10867236 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 15135530 | HCID 15135530 | 96.3% |
Reaction Steps
To a stirred mixture of 4 g of 2-amino-4,5-dimethoxybenzamide and 200 ml of ether was added dropwise, e solution of 3.3 g of benzoyl isothiocyanate in 100 ml of ether over 15 minutes. After 24 hours, the solid was collected, giving 7 g of the desired product as white crystals, mp 204°-207° C. (dec.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05001157 |
| Source dataset | uspto-grants-1991_03 |
| ORD ID | ord-11fb78b6fc6547419849e6d894fb8901 |
| Source note | uspto-grants-1991_03 |