HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Methylbenzoyl isothiocyanate → HCID 15135527, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Methylbenzoyl isothiocyanate | HCID 140139 | — |
| Reactant | 2-Amino-5-methylbenzamide | HCID 10329436 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 15135527 | HCID 15135527 | 91.7% |
Reaction Steps
To a stirred mixture of 3 g of 2-amino-5-methylbenzamide and 200 ml of ether was added dropwise, a solution of 3.7 g of 4-methylbenzoyl isothiocyanate in 100 ml of ether over 3 minutes. After 24 hours, the solid was collected, giving 6 g of the desired product as off-white crystals, mp 208°-209° C. (dec.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05001157 |
| Source dataset | uspto-grants-1991_03 |
| ORD ID | ord-4069010e62c24b25b7663212dfb2f6b7 |
| Source note | uspto-grants-1991_03 |