HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Methylbenzoyl isothiocyanate → HCID 15135529, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Methylbenzoyl isothiocyanate | HCID 141396 | — |
| Reactant | 2-Amino-N-methylbenzamide | HCID 308072 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 15135529 | HCID 15135529 | 93.4% |
Reaction Steps
To a stirred mixture of 5.4 g of 2-amino-N-methylbenzamide and 200 ml of ether was added dropwise, a solution of 6.67 g of 2-methylbenzoyl isothiocyanate in 100 ml of ether over 15 minutes. After several hours, the solid was collected, giving 11 g of the desired product as light grey crystals, mp 172°-175° C. (dec.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05001157 |
| Source dataset | uspto-grants-1991_03 |
| ORD ID | ord-4f705e92ca3c48d4a385297626b99830 |
| Source note | uspto-grants-1991_03 |