HuagongsheHuagongshe Chemistry Print Report · For research reference only
Allylamine → 2,2'-Azobis[n-(2-propenyl)-2-methylpropionamide]
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Allylamine | HCID 7853 | — |
| Reactant | 1,1'-Dimethyl 2,2'-(1,2-diazenediyl)bis(2-methylpropanoate) | HCID 75763 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 2,2'-Azobis[n-(2-propenyl)-2-methylpropionamide] | HCID 15724735 | — |
Reaction Steps
Dimethyl 2,2'-azobis(2-methylpropionate) in an amount of 41.9 g, 48 ml of methanol, and 43 g of a 28% CH3ONa methanol solution were mixed and stirred for dissolution, followed by dropwise addition of 25 g of allylamine to react at 19° to 21° C. for 20 hours.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05001228 |
| Source dataset | uspto-grants-1991_03 |
| ORD ID | ord-cbc849f2079f4b2e89bfcd0e603da8a8 |
| Source note | uspto-grants-1991_03 |