HCID 178511195, compound → HCID 178475040, compound

HRID 35964Notes

Reaction equation

HRID 35964 reaction equation
C([CH2:3][C:4]([NH:6][C@H:7]1[CH2:12][CH2:11][C@H:10]([O:13][N+:14]([O-:16])=[O:15])[CH2:9][CH2:8]1)=[O:5])#N.C(CC(N[C@H]1CC[C@H](O)CC1)=O)#N>>[C:4]([NH:6][C@H:7]1[CH2:8][CH2:9][C@H:10]([O:13][N+:14]([O-:16])=[O:15])[CH2:11][CH2:12]1)(=[O:5])[CH3:3]

Participants

3

Reactant 2

HCID 178511195HCID 178511195, compoundHCID 178511196HCID 178511196, compound

Product 1

HCID 178475040HCID 178475040, compoundYield 53%

Procedure

2-cyano-N-(trans-4-nitroxycyclohexyl)-acetic acid amide from 2-cyano-N-(trans-4-hydroxycyclohexyl)-acetic acid amide melting point: 149°-150° C. (ether), yield: 53% of theory.

Sources & evidence

ORD record
ord-ecd17fce5fe54de281b5939c329ed015
Source dataset
uspto-grants-1995_05
Patent number
US05411989

Reaction notes

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