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HRID359669

反应详情

EQUATION

反应方程式

HRID 359669 的结构方程式

REACTANTS

反应物

2
结构：C=Cc1ccc(S(=O)(=O)Cl)cc1
HCID9855777

4-Vinylbenzenesulfonyl chloride

C8H7ClO2S

结构：O=C1CC(c2ccccc2)C(=O)N1O
HCID12391645

未命名化合物

PRODUCTS

生成物

1
结构：C=Cc1ccc(S(=O)(=O)[O-])cc1.O=C1CC(c2ccccc2)C(=O)N1O
HCID86744681

未命名化合物

收率 115.6%

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CC(C)=O
溶剂HCID180

Acetone

C3H6O

PROCEDURE

实验过程

50 ml of acetone was added to 3.8 g of N-hydroxy-2-phenylsuccinimide and 4.1 g of p-styrenesulfonyl chloride and then the same procedure as that of Preparation Example 1 was repeated to obtain 4.3 g of N-hydroxy-2-phenylsuccinimide-p-styrenesulfonate.

WORKUP

后处理

  1. customthe same procedure as that of Preparation Example 1