Styrene-4-sulfonyl chloride → N-hydroxy-2-phenylsuccinimide p-styrenesulfonate

HRID 359669Notes

Reaction equation

HRID 359669 reaction equation
[OH:1][N:2]1[C:6](=[O:7])[CH2:5][CH:4]([C:8]2[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=2)[C:3]1=[O:14].[CH2:15]=[CH:16][C:17]1[CH:22]=[CH:21][C:20]([S:23](Cl)(=[O:25])=[O:24])=[CH:19][CH:18]=1>CC(C)=O>[OH:1][N:2]1[C:6](=[O:7])[CH2:5][CH:4]([C:8]2[CH:9]=[CH:10][CH:11]=[CH:12][CH:13]=2)[C:3]1=[O:14].[CH2:15]=[CH:16][C:17]1[CH:22]=[CH:21][C:20]([S:23]([O-:25])(=[O:1])=[O:24])=[CH:19][CH:18]=1

Participants

4

Reactant 2

HCID 9855777Styrene-4-sulfonyl chlorideHCID 12391645N-hydroxy-2-phenylsuccinimide

Product 1

HCID 86744681N-hydroxy-2-phenylsuccinimide p-styrenesulfonateYield 115.6%

Reagents, catalysts & solvents 1

HCID 180AcetoneSolvent

Procedure

50 ml of acetone was added to 3.8 g of N-hydroxy-2-phenylsuccinimide and 4.1 g of p-styrenesulfonyl chloride and then the same procedure as that of Preparation Example 1 was repeated to obtain 4.3 g of N-hydroxy-2-phenylsuccinimide-p-styrenesulfonate.

Workup

  1. customthe same procedure as that of Preparation Example 1

Sources & evidence

ORD record
ord-4f2cd66673a246afa7467404582ff84c
Source dataset
uspto-grants-1991_03
Patent number
US05002853

Reaction notes

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