HCID 178484862, compound → HCID 178523823, compound

HRID 35967Notes

Reaction equation

HRID 35967 reaction equation
C[N:2]([C@H:5]1[CH2:10][CH2:9][C@H:8]([O:11][N+:12]([O-:14])=[O:13])[CH2:7][CH2:6]1)[CH:3]=[O:4].CN[C@H]1CC[C@H](O[N+]([O-])=O)CC1>>[CH:3]([NH:2][C@H:5]1[CH2:10][CH2:9][C@H:8]([O:11][N+:12]([O-:14])=[O:13])[CH2:7][CH2:6]1)=[O:4]

Participants

3

Reactant 2

HCID 178484862HCID 178484862, compoundHCID 178485741HCID 178485741, compound

Product 1

HCID 178523823HCID 178523823, compoundYield 60%

Procedure

trans-N-methyl-N-formyl-4-nitroxycyclohexylamine from trans-N-methyl-4-nitroxycyclohexylamine melting point: 52°-54° C. (ether/isohexane), yield: 60% of theory.

Sources & evidence

ORD record
ord-b24ebc5c9e1b4814845e2e28f2770630
Source dataset
uspto-grants-1995_05
Patent number
US05411989

Reaction notes

Loading…