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HRID359672

反应详情

EQUATION

反应方程式

HRID 359672 的结构方程式

REACTANTS

反应物

2
结构：O=S(=O)(Cl)c1cccc2ccccc12
HCID66560

1-Naphthalenesulfonyl chloride

C10H7ClO2S

结构：O=C1C=CC(=O)N1O
HCID78535

1-Hydroxy-1H-pyrrole-2,5-dione

C4H3NO3

PRODUCTS

生成物

1
结构：O=C1C=CC(=O)N1O.O=S(=O)([O-])c1cccc2ccccc12
HCID86744683

未命名化合物

收率 135%

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CC(C)=O
溶剂HCID180

Acetone

C3H6O

PROCEDURE

实验过程

120 ml of acetone was added to 5.7 g of N-hydroxymaleimide and 11.3 g of 1-naphthalenesulfonyl chloride and then the same procedure as that of Preparation Example 1 was repeated to obtain 10.9 g of N-hydroxymaleimide-1-naphthalenesulfonate.

WORKUP

后处理

  1. customthe same procedure as that of Preparation Example 1