Dimethylamine → HCID 178513907, compound

HRID 35969Notes

Reaction equation

HRID 35969 reaction equation
O([C@H]1CC[C@H](C[NH:12][C:13](=[O:21])[CH2:14][CH2:15][C:16]([N:18](C)C)=[O:17])CC1)[N+]([O-])=O.[O:22]([C@H:26]1[CH2:31][CH2:30][C@H:29](CNC(=O)CCC(O)=O)[CH2:28][CH2:27]1)[N+:23]([O-:25])=[O:24].CNC>>[O:22]([C@H:26]1[CH2:27][CH2:28][C@H:29]([NH:12][C:13](=[O:21])[CH2:14][CH2:15][C:16]([NH2:18])=[O:17])[CH2:30][CH2:31]1)[N+:23]([O-:25])=[O:24]

Participants

4

Reactant 3

HCID 674DimethylamineHCID 178484541HCID 178484541, compoundHCID 178525516HCID 178525516, compound

Product 1

HCID 178513907HCID 178513907, compoundYield 40%

Procedure

N-(trans-4-nitroxycyclohexylmethyl)-N',N'-dimethylsuccinic acid diamide from N-(trans-4-nitroxycyclohexylmethyl)-succinic acid monoamide and dimethylamine melting point: 70°-71° C. (ether), yield: 40%

Sources & evidence

ORD record
ord-53e3efb172b94fd8a3e71b97f51acb92
Source dataset
uspto-grants-1995_05
Patent number
US05411989

Reaction notes

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