反应详情

A suspension of 3.4 g (20 mmol) of 2,3-dihydro--N,N,5-trimethyl-2-oxo-1H-imidazole-4-carboxamide (prepared in example 3) and 4.4 g cf phosphorus pentasulfide in 100 ml of dry pyridine is stirred at reflux temperature for 6 hours. The mixture is allowed to cool overnight and is diluted with water. The precipitate is collected and recrystallized from 50% aqueous ethanol to give the title compound.

1. temperatureat reflux temperature for 6 hours
2. temperatureto cool overnight
3. customThe precipitate is collected
4. customrecrystallized from 50% aqueous ethanol