HCID 54135160, compound → HCID 53699739, compound

HRID 359746Notes

Reaction equation

HRID 359746 reaction equation
[O:1]1[CH:5]=[CH:4][CH:3]=[C:2]1[CH:6]=[CH:7][CH2:8][CH2:9][CH2:10][C:11](O)=[O:12]>CCOCC>[O:1]1[CH:5]=[CH:4][CH:3]=[C:2]1[CH:6]=[CH:7][CH2:8][CH2:9][CH2:10][CH2:11][OH:12]

Participants

3

Reactant 1

HCID 54135160HCID 54135160, compound

Product 1

HCID 53699739HCID 53699739, compound

Reagents, catalysts & solvents 1

HCID 3283Diethyl EtherSolvent

Procedure

6-(2-Furyl)-5-hexenoic acid (3.6 g) in ether (25 ml) was reduced according to the method of Intermediate 15, except that the reaction time was 1.5 h, and there was no purification by FCC. The title compound was obtained as a pale yellow oil (2.89 g), t.l.c. (hexane-ether 1:1) Rf 0.17.

Workup

  1. customno purification by FCC

Sources & evidence

ORD record
ord-cb3295dfdede416da6bef3065bb6c5d3
Source dataset
uspto-grants-1991_03
Patent number
US05002966

Reaction notes

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