HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,5-Dimethyl-4-hydroxybenzaldehyde → 3,5-Dimethyl-4-[5-(3-methyl-5-isoxazolyl)pentyloxy]benzaldehyde
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,5-Dimethyl-4-hydroxybenzaldehyde | HCID 75222 | — |
| Reactant | 5-(5-Bromopentyl)-3-methylisoxazole | HCID 13544046 | — |
| Product | 3,5-Dimethyl-4-[5-(3-methyl-5-isoxazolyl)pentyloxy]benzaldehyde | HCID 14981836 | — |
| Product | Hexane isopropyl acetate | HCID 22034165 | — |
Reaction Steps
3,5-Dimethyl-4-[5-(3-methyl-5-isoxazolyl)pentyloxy]benzaldehyde was prepared from 3,5-dimethyl-4-hydroxybenzaldehyde and 5-(5-bromopentyl)-3-methylisoxazole according to the procedure of Example 96(a), and was obtained in 82% yield as a pale-orange solid, m.p. 51°-53° C. (from hexane-isopropyl acetate).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05002960 |
| Source dataset | uspto-grants-1991_03 |
| ORD ID | ord-40f2b9dc8e0b4ce1b77380b4450a1a30 |
| Source note | uspto-grants-1991_03 |