HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
3,4,6-Trifluoro-5-hydroxyphthalic acid → 2,4,5-Trifluoro-3-hydroxybenzoic Acid
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 3,4,6-Trifluoro-5-hydroxyphthalic acid | HCID 10198587 | — |
| Lösungsmittel | Water | HCID 962 | — |
| Produkt | 2,4,5-Trifluoro-3-hydroxybenzoic Acid | HCID 2734270 | — |
Reaktionsschritte
Japanese Patent Application 86/290399 as abstracted in Chem. Abstracts (CA109 (19) 170038e), discloses that 3,5,6-trifluoro-4-hydroxyphthalic acid may be decarboxylated by heating the compound for three hours, in water, under nitrogen atmosphere, at 140° C. (in a sealed tube) to yield 2,4,5-trifluoro-3-hydroxybenzoic acid.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05003103 |
| Quelldatensatz | uspto-grants-1991_03 |
| ORD ID | ord-02c5e3564f1648c7b7f6decf3e348f6e |
| Quellennotiz | uspto-grants-1991_03 |