Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Isatoic Anhydride → 1-Heptyl-3-Ethoxycarbonyl-4-Methoxy-2(1H)-Quinolinone
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Isatoic Anhydride | HCID 8359 | — |
| 반응물 | Diazomethane | HCID 9550 | — |
| 반응물 | 1-Heptyl-3-Ethoxycarbonyl-4-Hydroxy-2(1H)-Quinolinone | HCID 54684781 | — |
| 용매 | Diethyl Ether | HCID 3283 | — |
| 생성물 | 1-Heptyl-3-Ethoxycarbonyl-4-Methoxy-2(1H)-Quinolinone | HCID 21217803 | — |
반응 단계
Following the procedure set forth in Preparation A, steps (2-3), isatoic anhydride was converted to 1-heptyl-4-hydroxy-3-ethoxycarbonyl-2(1H)-quinolinone, which upon reaction with excess diazomethane in ether gave the title compound. That the expected product was obtained was confirmed by the spectral data: MS: m/e 345 (M+).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05412104 |
| 출처 데이터셋 | uspto-grants-1995_05 |
| ORD ID | ord-f2f1ff701b9b4467a519f5737562da63 |
| 출처 메모 | uspto-grants-1995_05 |