HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 361285Generated: October 30, 2026
Dimethylformamide → HCID 53741928, compound
https://huagongshe.com/reaction/361285
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Dimethylformamide | HCID 6228 | — |
| Reactant | Indoline | HCID 10328 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 1-Bromoheptane | HCID 12369 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 53741928 | HCID 53741928 | — |
Reaction Steps
A mixture of indoline (17 parts), 1-bromoheptane (31 parts), potassium carbonate (24 parts) and N,N-dimethylformamide (30 parts) was stirred at 100° C. for 3 days. The cooled mixture was diluted with toluene, washed with water (×4), dried (MgSO4) and evaporated to leave 1-heptyl-2,3-dihydro-1H-indole (30 parts).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US05865857 |
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| Source dataset | uspto-grants-1999_02 |
|---|
| ORD ID | ord-e7683a7bca05414b963ccfcfb0ec4f54 |
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| Source note | uspto-grants-1999_02 |
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