HRID36152
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
AUXILIARIES
试剂、催化剂与溶剂
PROCEDURE
实验过程
A solution of 840 mgs of 3-(5-benzyloxypentyl)(1-hexenyl)benzene in 25 mls of methanol is hydrogenated over 5% palladium on carbon and then filtered through celite, concentrated, and chromatographed over silica gel (3:2 ether:hexane) to yield pure 5-(3-hexylphenyl)-pentanol.
WORKUP
后处理
- filtrationfiltered through celite,
- concentrationconcentrated
- customchromatographed over silica gel (3:2 ether:hexane)