HRID36152

反应详情

EQUATION

反应方程式

HRID 36152 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

A solution of 840 mgs of 3-(5-benzyloxypentyl)(1-hexenyl)benzene in 25 mls of methanol is hydrogenated over 5% palladium on carbon and then filtered through celite, concentrated, and chromatographed over silica gel (3:2 ether:hexane) to yield pure 5-(3-hexylphenyl)-pentanol.

WORKUP

后处理

  1. filtrationfiltered through celite,
  2. concentrationconcentrated
  3. customchromatographed over silica gel (3:2 ether:hexane)