HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 86753651, compound → methyl 4,7-dimethoxy-1H-indole-2-carboxylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 86753651 | HCID 86753651 | — |
| Solvent | O-Xylene | HCID 7237 | — |
| Product | methyl 4,7-dimethoxy-1H-indole-2-carboxylate | HCID 4714975 | 74.7% |
Reaction Steps
A solution of 1.5 g (6.84 mmol) of the above-obtained methyl 2,5-dimethoxyphenyl-α-azidocinnamate in 300 ml of xylene was refluxed for 4 hours. After distilling off xylene, the residue was recrystallized from methanol to provide 1.01 g of the title compound (74.7%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05866594 |
| Source dataset | uspto-grants-1999_02 |
| ORD ID | ord-031bcfff8d504574be5d9be92800f607 |
| Source note | uspto-grants-1999_02 |