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HRID36167

反应详情

EQUATION

反应方程式

HRID 36167 的结构方程式

REACTANTS

反应物

2
结构：C=C(P(=O)(OCC)OCC)P(=O)(OCC)OCC
HCID11022954

Tetraethyl vinylidene phosphonate

C10H22O6P2

结构：COc1ccc2nc(NC(=O)CC(=O)c3ccccc3)sc2c1
HCID19975336

未命名化合物

PRODUCTS

生成物

1
结构：CCOP(=O)(OCC)C(CCC(=O)c1cccs1)P(=O)(OCC)OCC
HCID85643872

未命名化合物

PROCEDURE

实验过程

Ethenylidenebisphosphonic acid tetraethyl ester (I) ,and 2-acetylthiophene (II, 0.76 ml); MS (m/e) 426, 381, 315, 289, 261, 152 and 111; IR (neat) 1663, 1518, 1478, 1443, 1416, 1392, 1368, 1355, 1250, 1164 and 1142 cm-1 ; NMR (CDCl3) 7.77, 7.62, 7.12, 4.2, 3.32, 2.58, 2.36 and 1.33 67 ; CMR (CDCl3) 192, 144, 133.5, 135.5, 128, 62, 38, 32.5 (t), 20.5 and 16 δ.