O-ethylhydroxylamine hydrochloride → HCID 54360874, compound

HRID 361706Notes

Reaction equation

HRID 361706 reaction equation
[CH2:1]([CH:4]([CH2:14][O:15][CH2:16][CH2:17][CH2:18][NH:19][CH:20]([CH3:22])[CH3:21])[CH2:5][C:6]([C:8]1[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=1)=O)[CH:2]=[CH2:3].Cl.[CH2:24]([O:26][NH2:27])[CH3:25]>>[CH2:24]([O:26][N:27]=[C:6]([C:8]1[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=1)[CH2:5][CH:4]([CH2:1][CH:2]=[CH2:3])[CH2:14][O:15][CH2:16][CH2:17][CH2:18][NH:19][CH:20]([CH3:22])[CH3:21])[CH3:25]

Participants

3

Reactant 2

HCID 76850O-ethylhydroxylamine hydrochlorideHCID 54091471HCID 54091471, compound

Product 1

HCID 54360874HCID 54360874, compound

Procedure

The procedure described in Example 88 was repeated using 3-allyl-4-(3-[N-isopropylamino]propoxy)butyrophenone and ethoxyamine hydrochloride to give 3-allyl-4-(3-[N-isopropylamino)propoxy)-butyrophenone O-ethyloxime as a solid, m.p. 124°-126° C.

Sources & evidence

ORD record
ord-c132c3593d2d4aadb511610c6cf83f98
Source dataset
uspto-grants-1999_02
Patent number
US05866611

Reaction notes

Loading…