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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 361723Generated: November 1, 2026

Hydrochloric Acid → HCID 53867993, compound

https://huagongshe.com/reaction/361723

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydrochloric AcidHCID 313—
ReactantHCID 53647176HCID 53647176—
CatalystPalladiumHCID 23938—
SolventEthanolHCID 702—
ProductHCID 53867993HCID 5386799380.2%

Reaction Steps

A solution of N,N-diethyl-3-(3-benzyloxyphenoxy)propylamine (0.7 g) in ethanol was treated with ethereal hydrogen chloride solution and the mixture hydrogenated in the presence of Pd/C (0.25 g, 5% w/w) for 2 hours. The catalyst was removed by filtration and the filtrate evaporated. The residue was crystallised from a mixture of ethanol and ether to give N,N-diethyl-3-(3-hydroxyphenoxy)propylamine (0.4 g), m/z 223.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05866611
Source datasetuspto-grants-1999_02
ORD IDord-366dad1afe1c4f419113410fdb4c2b67
Source noteuspto-grants-1999_02