HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 53867993, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 53647176 | HCID 53647176 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 53867993 | HCID 53867993 | 80.2% |
Reaction Steps
A solution of N,N-diethyl-3-(3-benzyloxyphenoxy)propylamine (0.7 g) in ethanol was treated with ethereal hydrogen chloride solution and the mixture hydrogenated in the presence of Pd/C (0.25 g, 5% w/w) for 2 hours. The catalyst was removed by filtration and the filtrate evaporated. The residue was crystallised from a mixture of ethanol and ether to give N,N-diethyl-3-(3-hydroxyphenoxy)propylamine (0.4 g), m/z 223.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05866611 |
| Source dataset | uspto-grants-1999_02 |
| ORD ID | ord-366dad1afe1c4f419113410fdb4c2b67 |
| Source note | uspto-grants-1999_02 |