HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Phenylpiperazine → HCID 86753682, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Phenylpiperazine | HCID 7096 | — |
| Reactant | HCID 85172428 | HCID 85172428 | — |
| Product | HCID 86753682 | HCID 86753682 | 12% |
Reaction Steps
The same procedure as in Example 45 was performed with ethyl-N-(N-(4-cyano-2-fluorobenzoyl)-β-ethyl-α,α-dimethyl-β-alanyl)-4-piperidineacetate (1.48 g, 3.3 mmol) by using 1-phenylpiperazine (5.0 g) as an amine to yield the titled compound (237 mg, 12%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05866592 |
| Source dataset | uspto-grants-1999_02 |
| ORD ID | ord-d025a5963687449385a8689d6ea36725 |
| Source note | uspto-grants-1999_02 |