HRID361906

反应详情

EQUATION

反应方程式

HRID 361906 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

20.0 g of Ferulic acid was dissolved in 250 ml of methanol and subjected to catalytic reduction under normal pressure for 3 hours in the presence of 10% palladium carbon catalyst (50% wet type). After removing the catalyst by filtration, the resulting filtrate was concentrated to collect precipitated crystals by filtration, thereby obtaining 19.3 g of 3-(4-hydroxy-3-methoxy-phenyl)propionic acid.

WORKUP

后处理

  1. customAfter removing the catalyst
  2. filtrationby filtration
  3. concentrationthe resulting filtrate was concentrated
  4. customto collect
  5. customprecipitated crystals
  6. filtrationby filtration