huagongshe.com
HRID362039

反应详情

EQUATION

反应方程式

HRID 362039 的结构方程式

REACTANTS

反应物

2
结构：COc1ccc(CS[C@H]2C[C@@H](C(=O)N[C@@H]3CCNC3)N(C(=O)OCc3ccc([N+](=O)[O-])cc3)C2)cc1.Cl
HCID67586513

未命名化合物

结构：N=CNC(=O)OCc1ccc([N+](=O)[O-])cc1
HCID140386401

未命名化合物

PRODUCTS

生成物

1
结构：O=C(N=CN1CC[C@@H](NC(=O)[C@@H]2C[C@H](S)CN2C(=O)OCc2ccc([N+](=O)[O-])cc2)C1)OCc1ccc([N+](=O)[O-])cc1
HCID88299414

未命名化合物

收率 52.9%

PROCEDURE

实验过程

Following a procedure similar to that described in Preparations 23(iii) and 23(iv), but using 1.38 g of (2S,4S)-4-(4-methoxybenzylthio)-1-(4-nitrobenzyloxycarbonyl)-2-[(3R)-pyrrolidin-3-ylaminocarbonyl]pyrrolidine hydrochloride and 564 mg of N-(4-nitrobenzyloxycarbonyl)formamidine, 795 mg of the title compound were obtained as a powder.