HCID 15392197, compound → HCID 15392237, compound

HRID 362528Notes

Reaction equation

HRID 362528 reaction equation
[C:1]([O:5][C:6]([N:8]1[CH2:13][CH2:12][CH:11]([O:14][C:15]2[CH:34]=[CH:33][C:18]([NH:19][CH2:20][C:21]3[CH:30]=[C:29]4[C:24]([CH:25]=[CH:26][C:27]([C:31]#[N:32])=[CH:28]4)=[CH:23][CH:22]=3)=[CH:17][CH:16]=2)[CH2:10][CH2:9]1)=[O:7])([CH3:4])([CH3:3])[CH3:2].[C:35]([O:39][C:40](=[O:46])[NH:41][S:42](Cl)(=[O:44])=[O:43])([CH3:38])([CH3:37])[CH3:36]>>[C:1]([O:5][C:6]([N:8]1[CH2:13][CH2:12][CH:11]([O:14][C:15]2[CH:16]=[CH:17][C:18]([N:19]([CH2:20][C:21]3[CH:22]=[CH:23][C:24]4[C:29](=[CH:28][C:27]([C:31]#[N:32])=[CH:26][CH:25]=4)[CH:30]=3)[S:42]([NH:41][C:40](=[O:46])[O:39][C:35]([CH3:37])([CH3:36])[CH3:38])(=[O:43])=[O:44])=[CH:33][CH:34]=2)[CH2:10][CH2:9]1)=[O:7])([CH3:4])([CH3:2])[CH3:3]

Participants

3

Reactant 2

HCID 15392197HCID 15392197, compoundHCID 15677406tert-butyl N-(chlorosulfonyl)carbamate2×

Product 1

HCID 15392237HCID 15392237, compound

Procedure

Starting compound: 7-[[4-[(1-t-butoxycarbonyl-4-piperidyl)oxy]anilino]methyl]-2-naphthalenecarbonitrile, t-butyl(chlorosulfonyl)carbamate In this connection, the method for the synthesis of t-butyl(chlorosulfonyl)carbamate is described in Tetrahedron, 49(1), 65 (1993).

Sources & evidence

ORD record
ord-163cc8676787463da13692f062fb4c27
Source dataset
uspto-grants-1999_02
Patent number
US05869501

Reaction notes

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