Sulfuryl chloride → HCID 15766901, compound

HRID 362654Notes

Reaction equation

HRID 362654 reaction equation
[F:1][CH:2]([F:18])[O:3][C:4]1[N:8]([CH3:9])[N:7]=[C:6]([N:10]2[C:14]([CH3:15])=[C:13]([C:16]#[N:17])[CH:12]=[N:11]2)[CH:5]=1.S(Cl)([Cl:22])(=O)=O>C(Cl)Cl>[Cl:22][C:5]1[C:6]([N:10]2[C:14]([CH3:15])=[C:13]([C:16]#[N:17])[CH:12]=[N:11]2)=[N:7][N:8]([CH3:9])[C:4]=1[O:3][CH:2]([F:1])[F:18]

Participants

4

Reactant 2

HCID 24648Sulfuryl chlorideHCID 54402406HCID 54402406, compound

Product 1

HCID 15766901HCID 15766901, compound

Reagents, catalysts & solvents 1

HCID 6344DichloromethaneSolvent

Procedure

0.57 g (2.25 mmol) 1-(5-Difluoromethoxy-1-methyl-3-pyrazolyl)-5-methyl-4-pyrazolecarbonitrile was dissolved in 30 ml methylene chloride and at room temperature was treated with 0.30 g (2.25 mmol) sulfuryl chloride. The mixture was stirred for one hour and then concentrated.

Workup

  1. concentrationconcentrated

Sources & evidence

ORD record
ord-b62a304e28e54cc5a9b012d7f50fb3be
Source dataset
uspto-grants-1999_02
Patent number
US05869686

Reaction notes

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