Dichloromethane → HCID 23293649, compound

HRID 362859Notes

Reaction equation

HRID 362859 reaction equation
[F:1][C:2]1[CH:10]=[C:9]2[C:5]([CH:6]([CH3:15])[CH2:7]/[C:8]/2=[CH:11]\[C:12](O)=[O:13])=[CH:4][CH:3]=1.[Cl:16]CCl>>[F:1][C:2]1[CH:10]=[C:9]2[C:5]([CH:6]([CH3:15])[CH2:7]/[C:8]/2=[CH:11]\[C:12]([Cl:16])=[O:13])=[CH:4][CH:3]=1

Participants

3

Reactant 2

HCID 6344DichloromethaneHCID 23293638HCID 23293638, compound

Product 1

HCID 23293649HCID 23293649, compound

Procedure

This compound was prepared in an analogous manner to Example 15h with the replacement of (E)-2-(6-fluoro-3,3-dimethyl-1-indanylidene)acetic acid with (E)-2-(6-fluoro-3-methyl-1-indanylidene)acetic acid (9 g, 43.6 mmol). The product residue was dissolved in dichloromethane and used, without purification, in Example 17, 18, and 19.

Workup

  1. customused, without purification, in Example 17, 18, and 19

Sources & evidence

ORD record
ord-39f0ed87c6bc4379a8f2d4f487c90eb8
Source dataset
uspto-grants-1999_02
Patent number
US05872118

Reaction notes

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