HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triphenylphosphine → 4-Phenoxybutyltriphenylphosphonium bromide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triphenylphosphine | HCID 11776 | — |
| Reactant | (4-Bromobutoxy)benzene | HCID 70986 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | 4-Phenoxybutyltriphenylphosphonium bromide | HCID 49782785 | 81% |
Reaction Steps
Triphenylphosphine and 4-phenoxybutyl bromide were refluxed in benzene for 36 hours to yield triphenyl(4-phenoxybutyl)phosphonium bromide in 81% yield.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05872148 |
| Source dataset | uspto-grants-1999_02 |
| ORD ID | ord-1ec4144543534c8ead6d087172d17e35 |
| Source note | uspto-grants-1999_02 |