4-Hydroxybenzyl Alcohol → HCID 28561627, compound

HRID 363013Notes

Reaction equation

[OH:1][C:2]1[CH:9]=[CH:8][C:5]([CH2:6][OH:7])=[CH:4][CH:3]=1.[CH:10]1([CH2:16]Br)[CH2:15][CH2:14][CH2:13][CH2:12][CH2:11]1>>[CH:10]1([CH2:16][O:1][C:2]2[CH:9]=[CH:8][C:5]([CH2:6][OH:7])=[CH:4][CH:3]=2)[CH2:15][CH2:14][CH2:13][CH2:12][CH2:11]1

Participants

Reactant 2

HCID 1254-Hydroxybenzyl Alcohol

HCID 137636Cyclohexane, (bromomethyl)-

Product 1

HCID 28561627HCID 28561627, compound

Procedure

3-3 was prepared as described for the synthesis of 1-6 except 4-hydroxy-benzyl alcohol (3-1) and cyclohexylmethyl bromide (3-2) were used in Step A to yield 4-(cyclohexylmethoxy)benzyl alcohol directly. mp: 241°-3° C.;

Workup

custom3-3 was prepared

Sources & evidence

ORD record: ord-e0b3fd842aeb4787ab32b979ce75fdde
Source dataset: uspto-grants-1999_02
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05872138

Reaction notes

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