HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl 3-allyl-4-hydroxybenzoate → Methyl 4-hydroxy-3-propylbenzoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl 3-allyl-4-hydroxybenzoate | HCID 939882 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | Methyl 4-hydroxy-3-propylbenzoate | HCID 11805593 | — |
Reaction Steps
To 22-3 (6.0 g, 33.2 mmol) in 50 mL of EtOAc was added 60 mg of 5% Pd on carbon and the whole was hydrogenated at atmospheric pressure for 24 h. Hydrogen was removed from the reaction mixture and the solution was filtered through Celite. Evaporation of the solvent afforded product 22-4 as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05872138 |
| Source dataset | uspto-grants-1999_02 |
| ORD ID | ord-f01451e0f3f640d8932c8f76d798ecf0 |
| Source note | uspto-grants-1999_02 |