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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 363038Generated: October 25, 2026

Methyl 3-allyl-4-hydroxybenzoate → Methyl 4-hydroxy-3-propylbenzoate

https://huagongshe.com/reaction/363038

Reaction equation

Participants

RoleNameHCIDCharge
ReactantMethyl 3-allyl-4-hydroxybenzoateHCID 939882—
CatalystPalladiumHCID 23938—
SolventEthyl AcetateHCID 8857—
ProductMethyl 4-hydroxy-3-propylbenzoateHCID 11805593—

Reaction Steps

To 22-3 (6.0 g, 33.2 mmol) in 50 mL of EtOAc was added 60 mg of 5% Pd on carbon and the whole was hydrogenated at atmospheric pressure for 24 h. Hydrogen was removed from the reaction mixture and the solution was filtered through Celite. Evaporation of the solvent afforded product 22-4 as a white solid.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05872138
Source datasetuspto-grants-1999_02
ORD IDord-f01451e0f3f640d8932c8f76d798ecf0
Source noteuspto-grants-1999_02