Tributylvinyltin → HCID 53847754, compound

Participants

Reaction Conditions

Reaction Steps

To a solution of 23-3 (810 mg, 2.5 mmol) in 11.5 mL of dioxane was added 820 mg (2.6 mmol) of vinyltributyl tin followed by 58 mg (0.05 mmol) of Pd(PPh3)4. The resulting solution was then heated at 100° C. for 20 h. The solvent was distilled under reduced pressure and the residue was chromatographed to afford product 23-4.

Provenance & Evidence