HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 36320Generated: October 26, 2026
N-Methylbutylamine → N-butyl-N-methylacetamide dimethyl acetal
https://huagongshe.com/reaction/36320
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | N-Methylbutylamine | HCID 8068 | — |
| Reactant | 1,1-Dimethoxyethyl(dimethyl)amine | HCID 87835 | — |
| Product | N-butyl-N-methylacetamide dimethyl acetal | HCID 19379602 | — |
Reaction Steps
6.1 g (0.07 mol) of n-butylmethylamine are stirred with 9.3 g (0.07 mol) of N,N-dimethylacetamide dimethyl acetal for 24 hours under reflux at a bath temperature of 130° C. Subsequent vacuum distillation gives N-butyl-N-methylacetamide dimethyl acetal, bp 72°-75° C./31 mbar.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US05413994 |
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| Source dataset | uspto-grants-1995_05 |
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| ORD ID | ord-958d91a3e3b94844878d9825f3955bb5 |
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| Source note | uspto-grants-1995_05 |
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