HCID 10491019, compound → HCID 10904836, compound

HRID 363306Notes

Reaction equation

HRID 363306 reaction equation
NC1C=C(C2SC3C=CC=CC=3N=2)C([O:8][S:9]([C:12]([F:15])([F:14])[F:13])(=[O:11])=[O:10])=CC=1.[N:25]([C:28]1[CH:33]=[CH:32][C:31]([C:34]2[S:35][C:36]3[CH:42]=[CH:41][CH:40]=[CH:39][C:37]=3[N:38]=2)=[CH:30][CH:29]=1)=[N+]=[N-]>>[NH2:25][C:28]1[CH:33]=[CH:32][C:31]([C:34]2[S:35][C:36]3[CH:42]=[CH:41][CH:40]=[CH:39][C:37]=3[N:38]=2)=[CH:30][C:29]=1[O:11][S:9]([C:12]([F:15])([F:14])[F:13])(=[O:10])=[O:8]

Participants

3

Reactant 2

HCID 10491019HCID 10491019, compoundHCID 10571424HCID 10571424, compound

Product 1

HCID 10904836HCID 10904836, compoundYield 12%

Procedure

This compound was prepared in a similar way to the compound of Example XIV from 2-(4-azidophenyl)benzothiazole. The yield was 12%, (Found: M+ 374. C14H9F3N2O3S2 requires MW 374).

Sources & evidence

ORD record
ord-b08601304b454ebd960cd7598d9052d8
Source dataset
uspto-grants-1999_02
Patent number
US05874431

Reaction notes

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