2,3-Diaminopyridine → HCID 15772576, compound

HRID 363735Notes

Reaction equation

HRID 363735 reaction equation
NC1C(N)=CC=CN=1.[N:9]1[CH:14]=[CH:13][CH:12]=[CH:11][C:10]=1[C:15]1[C:24]([C:25]2[CH:30]=[CH:29][CH:28]=[CH:27][N:26]=2)=[N:23][C:22]2[C:17](=[CH:18][CH:19]=[N:20][CH:21]=2)[N:16]=1>>[N:9]1[CH:14]=[CH:13][CH:12]=[CH:11][C:10]=1[C:15]1[C:24]([C:25]2[CH:30]=[CH:29][CH:28]=[CH:27][N:26]=2)=[N:23][C:22]2[C:21](=[N:20][CH:19]=[CH:18][CH:17]=2)[N:16]=1

Participants

3

Procedure

The preparation of 62 is identical to that of 61 substituting 2,3-diaminopyridine for 3,4-diamino pyridine (Example K), giving 900 mg of the title compound as a white solid.

Sources & evidence

ORD record
ord-f32a340e769c45348aad5855ab6268db
Source dataset
uspto-grants-1999_02
Patent number
US05874587

Reaction notes

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