(Aminomethyl)phosphonic acid → Glyphosate

HRID 363809Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 363809
[NH2:1][CH2:2][P:3](=[O:6])([OH:5])[OH:4].O.[C:8]([OH:12])(=[O:11])[CH:9]=O.[H][H]>>[CH2:9]([NH:1][CH2:2][P:3]([OH:5])([OH:4])=[O:6])[C:8]([OH:12])=[O:11]

Komponenten

4

Edukt 3

HCID 14017(Aminomethyl)phosphonic acidHCID 15620607Glyoxylic acid, monohydrateHCID 178418361HCID 178418361, Verbindung

Produkt 1

HCID 3496GlyphosateAusbeute 96 %

Versuchsvorschrift

Aminomethylphosphonic acid and glyoxylic acid hydrate were reacted under catalytic hydrogenation conditions in the manner described in Example 2, except prior to introduction of hydrogen, the pH was adjusted to 8.0. A 96% yield of glyphosate was obtained.

Quellen und Nachweise

ORD-Eintrag
ord-aa2d357ff23046789b5dfc6ba8ce96a7
Quelldatensatz
uspto-grants-1999_02
Patentnummer
US05874612

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