HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Mercapto-2-propanol → HCID 15295172, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Mercapto-2-propanol | HCID 102545 | — |
| Reactant | HCID 53793465 | HCID 53793465 | — |
| Product | HCID 15295172 | HCID 15295172 | 97.5% |
Reaction Steps
11.5 g (0.057 mol) of 2-nitro-4-amino-5-chloro-N-(methyl)aniline and 7.8 g (0.085 mol) of 1-mercaptopropan-2-ol were used as the starting materials to give dark brown crystals (14.3 g) melting at 152° C. (recrystallization from 96° ethanol) whose elemental analysis calculated for C10H15N3O3S was:
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05874618 |
| Source dataset | uspto-grants-1999_02 |
| ORD ID | ord-81abc15025a342188069438264b3853a |
| Source note | uspto-grants-1999_02 |